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921-03-9 Didara to gaju 1,1,3-Trichloroacetone olupese ni Ilu China

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CAS: 921-03-9, 1,1,3-Trichloroacetone fun olupese elegbogi ni China.Ni iṣura.
921-03-9
Didara to gaju 1,1,3-Trichloroacetone olupese ni Ilu China
1,1,3-Trichloroacetone/didara to gaju/owo to dara julọ CAS NO.921-03-9 CAS NO.921-03-9
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  • Orukọ ọja:1,1,3-Trichloroacetone
  • CAS:921-03-9
  • MF:C3H3Cl3O
  • MW:67.52
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    Ohun elo

    Awọn alaye kiakia

    • Orukọ Pro:Didara to gaju 1,1,3-Trichloroacetone su...
    • CasNo:921-03-9
    • Fọọmu Molecular:C3H3Cl3O
    • Ìfarahàn:omi ti ko ni awọ funfun tabi omi ti ko ni awọ (...
    • Ohun elo:Agbedemeji
    • Akoko Ifijiṣẹ:O wa
    • Idipo:25kgs / okun ilu tabi 200kgs / UN ilu
    • Ibudo:Shanghai
    • Agbara iṣelọpọ:30 Metiriki Toonu / osù
    • Mimo:99%
    • Ibi ipamọ:ni itura ati ki o gbẹ ibi
    • Gbigbe:nipasẹ okun tabi nipasẹ afẹfẹ
    • Nọmba Iwọn:1 Metiriki Toonu
    • Irin ti o wuwo:tọka si COA
    • tọka si COA:tọka si COA

     

    1,1,3-Trichloroacetone/didara to gaju/owo to dara julọ CAS NO.921-03-9 CAS NO.921-03-9

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    Sipesifikesonu

    Orukọ ọja 1,3,3-trichloroacetone
    2-Propanone, 1,1,3-trichloro-
    1,1,3-trichloropropan-2-ọkan
    1,1,3-Trichloroacetone
    EINECS 213-063-6
    MFCD00040500
    Oja Ile-iṣẹ naa ni ọpọlọpọ ninu akojo ọja iṣura, ati pe o le ṣeto gbigbe ni akoko.
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    N-Benzyl-N-ethylaniline Dye intermediates. Used to make acidic light green SF and other blue dyes.
    Crystal violet lactone45

    Ipele mimọ-giga ti igbaradi 1,1,3-trichloroacetone

    Áljẹbrà: acetone catalyzed kiloraidi ati ti a ṣe nipasẹ crystallization epo ni 1,1,3-trichloroacetone pẹlu mimọ giga ti ko kere ju 99.0%, pẹlu ikore ti 45%

    -----.Ọrọ Iṣaaju

    1,1,3■trichloroacetone jẹ agbedemeji pataki ninu iṣelọpọ folic acid.Ni bayi, 1,1,3.acetone trichloropacetone, gigun iṣelọpọ gigun (wakati 48), yiyan ti ko dara, ikore kekere, 1,1,3- trichloropacetone akoonu jẹ nikan nipa 17%, lẹhin ti omi isediwon, awọn oniwe-akoonu jẹ nikan 51.9% .Ati awọn gbóògì iye owo ti wa ni ga, awọn ọja atunse ti wa ni kekere.These gbogbo ja si ga abele folic acid gbóògì iye owo, soro lati mu awọn akoonu ati awọn miiran. Awọn iṣoro.Onkọwe ka nọmba nla ti awọn iwe-ipamọ ati ajeji.Lẹhin ọpọlọpọ awọn idanwo ati awọn ijinlẹ, a ṣafikun ayase ati iṣakoso iyara fou chlorine, idinku akoko ifaseyin si 1,1,3-3 trichloropacetone ni awọn wakati 24, ati 1,1,3-3 trichloropacetone crystallization pẹlu mimọ ti o tobi ju 99% ati awọn ikore ti o ju 45%.

    II.Apa idanwo

    1. lenu

    0000

    1. II.

      CHACCha+Cl:—ClCH.2CCH.3+ Cl.2CHCCH.3+C1CH.2CCH.2C1+

    1. Awọn igbesẹ idanwo

    Ninu ọpọn ọrun mẹrin pẹlu condenser iyipo 500ml, iye kan ti acetone ati ayase ni a mu soke ati jẹun si chlorine ni iwọn otutu ifa ti 10 ~ 30 W.Bẹrẹ akoko, da gbigbe nipasẹ chlorine ni awọn wakati pupọ lẹhin iṣesi, ati tẹsiwaju gbigbọn fun wakati 1. A ṣe afikun epo pataki bi ohun elo ti a fi kun si adalu ti o ni abajade, ti a fi fun wakati 1 nigba ti o tutu si 10 ° C crystallization, ti o nmu 1,1,3-trichloroacetone jade.

    1. 1,1,3.Ipinnu yiyan ti trichloroacetone ti nw

    Varin 3700 gaasi chromatograph, iwe kikun QF1 ati aṣawari FID ni a lo lati yan yiyan èrè mimọ ti ọja ati ojutu kiloraidi.

    1. Awọn abajade ti ijiroro naa
    2. Ipa ti ayase lori yiyan kiloraidi ṣe afihan yiyan ti chlorination acetone

    Ipa nla,Table 1 ṣe atokọ akojọpọ awọn abajade esiperimenta kan.Lati tabili 1, yiyan ti o kere ju ti 1,1,3-trichloroacetone ti pọ si ni pataki (nipa 19.1%) laisi ayase, ati

      yellow amine catalyst jẹ ohun ti o dara julọ, to 57.5% o. Awọn ipo idanwo: Innl acetone, 3nr) l chlorine, ayase 0.6g, iwọn otutu 1030°C,

    akoko 18 wakati. Laarin 12 wakati va: 3.9 Cao h; 2

    〜 7 wakati, vq: 27 Cao h; 7 - 18 wakati, VQ: 3.9 si h.Table 1. Awọn ipa ti ayase lori yiyan ọja

    1. Ipa ti iyara nipasẹ-chlorine lori iṣesi naa

    Idanwo naa rii pe chlorine aṣọ ni yiyan ọja ti ko dara, ni pataki imudarasi yiyan ọja ati ikore.

     

     

     

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